Examples of TG/DTA analysis
The TG-DTA analysis for Clay 4 is typical of disordered kaolin with total weight loss of about 11.0%.
Peak/°C | Reaction |
99.2 | Loss of physical adsorbed water |
340.8 | Weight loss due to decomposition of organic content |
550.0 | Dehydroxylation of kaolin to metakaollin |
951.2 | Transformation of metakaolin to spinel |
Generally, the corresponding weight loss due to the dehydroxylation of kaolin to metakaolin gives an indication of the amount of clay minerals that are present in the sample. A pure kaolin sample has a theoretical weight loss of 13.9%.
The degree of sharpness of the last peak, Peak A and Peak B gives an idea of the orderliness of the kaolin structure. Clay 3 is a well- ordered kaolin as Peak A is narrow and sharp while Clay 4 is a disordered kaolin as Peak B appears broad. The orderliness of the kaolin structure affects the clay's dry strength. Generally disordered clays have higher dry strength than well-ordered ones.